{"id":1836,"date":"2021-06-21T10:47:46","date_gmt":"2021-06-21T01:47:46","guid":{"rendered":"https:\/\/www.agr.kyushu-u.ac.jp\/shien_new\/?page_id=1836"},"modified":"2024-06-21T16:37:21","modified_gmt":"2024-06-21T07:37:21","slug":"%e9%ab%98%e9%80%9f%e6%b6%b2%e4%bd%93%e3%82%af%e3%83%ad%e3%83%9e%e3%83%88%e3%82%b0%e3%83%a9%e3%83%95%e8%b3%aa%e9%87%8f%e5%88%86%e6%9e%90%e8%a3%85%e7%bd%ae-lcms-it-tof","status":"publish","type":"page","link":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/%e9%81%8b%e7%94%a8%e6%a9%9f%e5%99%a8\/%e5%a4%a7%e5%9e%8b%e6%a9%9f%e5%99%a8\/%e9%ab%98%e9%80%9f%e6%b6%b2%e4%bd%93%e3%82%af%e3%83%ad%e3%83%9e%e3%83%88%e3%82%b0%e3%83%a9%e3%83%95%e8%b3%aa%e9%87%8f%e5%88%86%e6%9e%90%e8%a3%85%e7%bd%ae-lcms-it-tof","title":{"rendered":"\u9ad8\u901f\u6db2\u4f53\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u8cea\u91cf\u5206\u6790\u88c5\u7f6e LCMS-IT-TOF"},"content":{"rendered":"\n

\u9ad8\u901f\u6db2\u4f53\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u8cea\u91cf\u5206\u6790\u88c5\u7f6e LCMS-IT-TOF<\/h2>\n\n\n\n

\u6982\u8981<\/h3>\n\n\n\n
\n
\n
\u30e1\u30fc\u30ab\u30fc<\/td>\u5cf6\u6d25\u88fd\u4f5c\u6240<\/td><\/tr>
\u8a2d\u7f6e\u5834\u6240<\/td>\u30a6\u30a8\u30b9\u30c85\u53f7\u9928305\u5ba4<\/td><\/tr>
\u62c5\u5f53\u8005<\/td>\u8d64\u5742<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n
\u5229\u7528\u4e8b\u4f8b\u8ad6\u6587\u30ea\u30b9\u30c8<\/a><\/pre>\n<\/div>\n\n\n\n
\n
\"\"<\/a><\/figure>\n<\/div>\n<\/div>\n\n\n\n
\u7279\u8272<\/h3>\n\n\n\n
\u9ad8\u7cbe\u5ea6MSn\u6e2c\u5b9a\u3001\u6b63\u8ca0\u30a4\u30aa\u30f3\u9ad8\u901f\u5207\u63db\u6e2c\u5b9a\u304c\u53ef\u80fd\u3002\u7cbe\u5bc6\u8cea\u91cf\u6e2c\u5b9a\u80fd\u304c\u9ad8\u304f\u3001\u5206\u5b50\u30a4\u30aa\u30f3\u53ca\u3073\u30d5\u30e9\u30b0\u30e1\u30f3\u30c8\u30a4\u30aa\u30f3\u306e\u5206\u5b50\u7d44\u6210\u63a8\u5b9a\u304c\u53ef\u80fd\u3067\u3042\u308b\u305f\u3081\u3001\u4ee3\u8b1d\u7269\u30d7\u30ed\u30d5\u30a1\u30a4\u30ea\u30f3\u30b0\u3084\u30d0\u30a4\u30aa\u30de\u30fc\u30ab\u30fc\u63a2\u7d22\u306e\u5206\u91ce\u306b\u3082\u6709\u7528\u3067\u3042\u308b\u3002<\/pre>\n\n\n\n
\u4e88\u7d04\u30da\u30fc\u30b8<\/h3>\n\n\n\n
https:\/\/reservation.shareaid.kyushu-u.ac.jp\/ja\/mypage\/reservation\/1488<\/a><\/pre>\n\n\n\n
\u4e3b\u306a\u4ed5\u69d8<\/h3>\n\n\n\n
MS\u90e8<\/strong><\/td>LCMS-IT-TOF<\/strong><\/td><\/tr>
\u8cea\u91cf\u7bc4\u56f2<\/strong><\/td>m\/z 50\uff5e5,000<\/td><\/tr>
\u5206\u89e3\u80fd<\/strong><\/td>10,000 (FWHM at m\/z 1,000)<\/td><\/tr>
\u8cea\u91cf\u6e2c\u5b9a\u7cbe\u5ea6<\/strong><\/td>< 5 ppm (\u5185\u90e8\u6a19\u6e96\u6cd5)\uff0c < 20 ppm (\u5916\u90e8\u6a19\u6e96\u6cd5)<\/td><\/tr>
\u30b9\u30da\u30af\u30c8\u30eb\u6e2c\u5b9a\u5468\u671f<\/strong><\/td>10\u30b9\u30da\u30af\u30c8\u30eb\/sec<\/td><\/tr>
\u6b63\u8ca0\u5207\u66ff\u6642\u9593<\/strong><\/td>100 msec<\/td><\/tr>
MSn\u6e2c\u5b9a<\/strong><\/td>n = 10 \u307e\u3067\u8a2d\u5b9a\u53ef\u80fd<\/td><\/tr>
\u30a4\u30aa\u30f3\u6e90<\/strong><\/td>ESI<\/td><\/tr>
HPLC\u90e8<\/strong><\/td>Prominence<\/strong><\/td><\/tr>
\u30dd\u30f3\u30d7<\/strong><\/td>LC-20AD\uff082\u30dd\u30f3\u30d7\u9ad8\u5727\u30b0\u30e9\u30b8\u30a8\u30f3\u30c8\u30b7\u30b9\u30c6\u30e0\uff09<\/td><\/tr>
\u8131\u6c17\u30e6\u30cb\u30c3\u30c8<\/strong><\/td>DGU-20A5<\/td><\/tr>
\u30aa\u30fc\u30c8\u30b5\u30f3\u30d7\u30e9<\/strong><\/td>SIL-20AC \uff08\u30b5\u30f3\u30d7\u30eb\u30af\u30fc\u30e9\u30fc\u642d\u8f09\uff09<\/td><\/tr>
\u30ab\u30e9\u30e0\u30aa\u30fc\u30d6\u30f3<\/strong><\/td>CTO-20A \uff08\u5ba4\u6e29-10\u2103\u304b\u3089\u8a2d\u5b9a\u53ef\uff09<\/td><\/tr>
\u691c\u51fa\u5668<\/strong><\/td>SPD-20A\uff08UV 2\u6ce2\u9577\u691c\u51fa\uff09<\/td><\/tr>
\u30bd\u30d5\u30c8\u30a6\u30a7\u30a2<\/strong><\/td>LCMSsolution version 3.81<\/td><\/tr><\/tbody><\/table><\/figure>\n\n\n\n
\u30d5\u30ed\u30fc\u30a4\u30f3\u30b8\u30a7\u30af\u30b7\u30e7\u30f3\uff08In-fusion\uff09\u6e2c\u5b9a\u3082\u53ef\u80fd\u3067\u3059\u304c\u3001\u4e8b\u524d\u306b\u62c5\u5f53\u8077\u54e1\u306b\u3054\u76f8\u8ac7\u304f\u3060\u3055\u3044\u3002<\/pre>\n\n\n\n
\u3054\u5229\u7528\u65b9\u6cd5\u30fb\u6ce8\u610f\u4e8b\u9805<\/h3>\n\n\n\n
\n
\n
\u4f9d\u983c\u6e2c\u5b9a\uff08\u5206\u6790\u3092\u4f9d\u983c\u3059\u308b\u5834\u5408\uff09<\/a><\/p>\n<\/div>\n\n\n\n
\n
\u81ea\u4e3b\u6e2c\u5b9a\uff08\u88c5\u7f6e\u3092\u3054\u5229\u7528\u306e\u5834\u5408\uff09<\/a><\/p>\n<\/div>\n<\/div>\n\n\n\n
\u4f9d\u983c\u6e2c\u5b9a\uff08\u5206\u6790\u3092\u4f9d\u983c\u3059\u308b\u5834\u5408\uff09<\/h4>\n\n\n\n
\u4f9d\u983c\u6e2c\u5b9a\u306e\u3054\u5229\u7528\u65b9\u6cd5<\/h4>\n\n\n\n
\u4e8b\u524d\u306b\u304a\u6253\u3061\u5408\u308f\u305b\u306e\u4e0a\u3001ShareAid\u4e88\u7d04\u30fb\u7ba1\u7406\u30b7\u30b9\u30c6\u30e0\u3088\u308a\u5206\u6790\u4f9d\u983c\u3092\u7533\u8acb\u304f\u3060\u3055\u3044\u3002\u30b5\u30f3\u30d7\u30eb\u306f\u30a6\u30a8\u30b9\u30c85\u53f7\u9928312\u5ba4\u306b\u3054\u63d0\u51fa\uff08\u53c8\u306f\u3054\u9001\u4ed8\uff09\u304f\u3060\u3055\u3044\u3002<\/pre>\n\n\n\n
\u6e2c\u5b9a\u6599\u91d1<\/h4>\n\n\n\n
11,000\u5186\uff0f\u30b5\u30f3\u30d7\u30eb\n\u539f\u5247\u3068\u3057\u3066\u8cea\u91cf\u30c7\u30fc\u30bf\u304c\u5f97\u3089\u308c\u306a\u304b\u3063\u305f\u5834\u5408\u306b\u3082\u8ab2\u91d1\u3044\u305f\u3057\u307e\u3059\u3002\n\u6e2c\u5b9a\u306b\u306f1\uff5e2\u9031\u9593\u304b\u304b\u308a\u307e\u3059\u3002\u6a5f\u5668\u30e1\u30f3\u30c6\u30ca\u30f3\u30b9\u7b49\u3067\u5b8c\u4e86\u307e\u3067\u304a\u6642\u9593\u3092\u3044\u305f\u3060\u304f\u5834\u5408\u3082\u3042\u308a\u307e\u3059\u3002<\/pre>\n\n\n\n
\u6e2c\u5b9a\u30b5\u30f3\u30d7\u30eb\u306b\u3064\u3044\u3066<\/h4>\n\n\n\n
\u6e2c\u5b9a\u30b5\u30f3\u30d7\u30eb\u306fHPLC\u6e2c\u5b9a\u7d14\u5ea6\u306e\u3082\u306e\u306b\u9650\u308a\u307e\u3059\uff08\u30ab\u30e9\u30e0\u304a\u3088\u3073\u8cea\u91cf\u5206\u6790\u88c5\u7f6e\u3078\u306e\u30c0\u30e1\u30fc\u30b8\u3092\u8efd\u6e1b\u3059\u308b\u305f\u3081\uff09\u3002\n\u30b5\u30f3\u30d7\u30eb\u91cf\u306f\u30bf\u30f3\u30d1\u30af\u8cea\u6d88\u5316\u7269 \u6570pmol\u4ee5\u4e0a\u304c\u76ee\u5b89\u3067\u3059\u3002\u305d\u308c\u4ee5\u4e0b\u306e\u5834\u5408\u306f\u3054\u76f8\u8ac7\u304f\u3060\u3055\u3044\u3002<\/pre>\n\n\n\n
\u5206\u6790\u6761\u4ef6\u306b\u3064\u3044\u3066<\/h4>\n\n\n\n
\u4f9d\u983c\u6e2c\u5b9a\u3067\u306fHPLC\u306e\u6761\u4ef6\u691c\u8a0e\u306f\u539f\u5247\u3068\u3057\u3066\u884c\u3044\u307e\u305b\u3093\u3002\u3054\u6307\u793a\u3044\u305f\u3060\u3044\u305fHPLC\u6761\u4ef6\u3067\u306e\u307f\u6e2c\u5b9a\u81f4\u3057\u307e\u3059\u3002\u8a73\u3057\u304f\u306f\u304a\u554f\u3044\u5408\u308f\u305b\u304f\u3060\u3055\u3044\u3002<\/pre>\n\n\n\n
\u81ea\u4e3b\u6e2c\u5b9a\uff08\u88c5\u7f6e\u3092\u3054\u5229\u7528\u306e\u5834\u5408\uff09<\/h4>\n\n\n\n
\u5229\u7528\u6599\u91d1<\/h4>\n\n\n\n
1,300\u5186\/\u6642\u9593<\/pre>\n\n\n\n
\u6e2c\u5b9a\u30b5\u30f3\u30d7\u30eb\u306b\u3064\u3044\u3066<\/h4>\n\n\n\n
\u30b5\u30f3\u30d7\u30eb\u306f\u9069\u5207\u306a\u524d\u51e6\u7406\u3092\u884c\u3044\u3001\u30d5\u30a3\u30eb\u30bf\u30fc\u51e6\u7406\u7b49\u3067\u56fa\u5f62\u7269\u306f\u5168\u3066\u53d6\u308a\u9664\u3044\u3066\u304f\u3060\u3055\u3044\u3002\u691c\u51fa\u5668\u3084\u30a4\u30f3\u30bf\u30fc\u30d5\u30a7\u30a4\u30b9\u3078\u306e\u6b8b\u5b58\u3092\u3067\u304d\u308b\u3060\u3051\u9632\u3050\u305f\u3081\u3001\u8a66\u6599\u5c0e\u5165\u91cf\u304c\u591a\u304f\u306a\u3089\u306a\u3044\u3088\u3046\u3054\u691c\u8a0e\u304f\u3060\u3055\u3044\u3002<\/pre>\n\n\n\n
\u79fb\u52d5\u76f8\u306b\u3064\u3044\u3066<\/h4>\n\n\n\n
\u79fb\u52d5\u76f8\u306b\u306f\u30ea\u30f3\u9178\u5869\u7b49\u306e\u4e0d\u63ee\u767a\u6027\u306e\u5869\u306fMS\u90e8\u3067\u6790\u51fa\u3059\u308b\u305f\u3081\u3054\u5229\u7528\u3067\u304d\u307e\u305b\u3093\uff08HPLC\u306e\u307f\u306e\u5229\u7528\u3067\u3042\u3063\u3066\u3082\u4e0d\u53ef\uff09\u3002\u5869\u306e\u6790\u51fa\u3092\u9632\u3050\u305f\u3081\u3001\u4f7f\u7528\u524d\u5f8c\u306b\u5869\u306a\u3057\u306e\u79fb\u52d5\u76f8\u3067\u901a\u6db2\u3059\u308b\u3053\u3068\u3092\u304a\u9858\u3044\u3057\u3066\u3044\u307e\u3059\u3002\u306a\u304a\u3001\u30a4\u30aa\u30f3\u30da\u30a2\u8a66\u85ac\u306e\u3054\u5229\u7528\u306f\u5805\u304f\u304a\u65ad\u308a\u3055\u305b\u3066\u3044\u305f\u3060\u304d\u307e\u3059\u3002<\/span><\/pre>\n\n\n\n
\u88c5\u7f6e\u5229\u7528\u6642\u306e\u6d88\u8017\u54c1\u306b\u3064\u3044\u3066<\/h4>\n\n\n\n
\u30ab\u30e9\u30e0\u3001\u79fb\u52d5\u76f8\u3001\u30b5\u30f3\u30d7\u30eb\u30d0\u30a4\u30a2\u30eb\u306f\u5404\u81ea\u3054\u6e96\u5099\u306e\u4e0a\u3001\u3054\u5229\u7528\u5f53\u65e5\u306b\u304a\u6301\u3061\u8fbc\u307f\u304f\u3060\u3055\u3044\u3002\u304a\u6301\u3061\u8fbc\u307f\u3044\u305f\u3060\u304f\u7269\u54c1\u306e\u30bb\u30f3\u30bf\u30fc\u3067\u306e\u4fdd\u7ba1\u306f\u539f\u5247\u304a\u65ad\u308a\u3044\u305f\u3057\u307e\u3059\u3002<\/pre>\n","protected":false},"excerpt":{"rendered":"
\u9ad8\u901f\u6db2\u4f53\u30af\u30ed\u30de\u30c8\u30b0\u30e9\u30d5\u8cea\u91cf\u5206\u6790\u88c5\u7f6e LCMS-IT-TOF \u6982\u8981 \u30e1\u30fc\u30ab\u30fc \u5cf6\u6d25\u88fd\u4f5c\u6240 \u8a2d\u7f6e\u5834\u6240 \u30a6\u30a8\u30b9\u30c85\u53f7\u9928305\u5ba4 \u62c5\u5f53\u8005 \u8d64\u5742 \u5229\u7528\u4e8b\u4f8b\u8ad6\u6587\u30ea\u30b9\u30c8 \u7279\u8272 \u9ad8\u7cbe\u5ea6MSn\u6e2c\u5b9a\u3001\u6b63\u8ca0\u30a4\u30aa\u30f3\u9ad8\u901f\u5207\u63db\u6e2c\u5b9a\u304c\u53ef\u80fd\u3002\u7cbe\u5bc6\u8cea\u91cf\u6e2c […]<\/p>\n","protected":false},"author":8,"featured_media":1837,"parent":1498,"menu_order":3,"comment_status":"closed","ping_status":"closed","template":"","meta":{"vkexunit_cta_each_option":"","_expiration-date-status":"","_expiration-date":0,"_expiration-date-type":"","_expiration-date-categories":[],"_expiration-date-options":[]},"_links":{"self":[{"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/pages\/1836"}],"collection":[{"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/users\/8"}],"replies":[{"embeddable":true,"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/comments?post=1836"}],"version-history":[{"count":13,"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/pages\/1836\/revisions"}],"predecessor-version":[{"id":11132,"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/pages\/1836\/revisions\/11132"}],"up":[{"embeddable":true,"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/pages\/1498"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/media\/1837"}],"wp:attachment":[{"href":"https:\/\/www.agr.kyushu-u.ac.jp\/shien\/wp-json\/wp\/v2\/media?parent=1836"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}